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Research Articles

Vacuum Impregnation of Solid Lubricant as a Versatile Tool for Producing Self-Replenishable Solid Lubrication

ORCID Icon, , , , & ORCID Icon
Pages 33-46 | Received 14 Jul 2023, Accepted 17 Nov 2023, Published online: 03 Jan 2024
 

Abstract

Self-replenishable ways of applying solid lubrication in tribological systems are limited to the use of sintered self-lubricating composites. These are obtained by mixing solid lubricants with metallic powders or by the in situ precipitation of the lubricating phase. Both techniques can produce self-lubricating composites able to promote low friction coefficients in dry sliding conditions. However, the combination of solid lubricant and matrix is limited by the thermodynamic interactions during sintering. Filling the pores of sintered parts with solid lubricants by vacuum impregnation is a versatile way to promote solid lubrication, allowing any combination of solid lubricant and matrix to be used, avoiding deleterious phases and other sintering problems typical in sintered self-lubricating composites. In this work, low alloy sintered steel was produced by mixing Astaloy CRL powders with 0.6 wt% C, the sintered specimens were impregnated with graphite (1.10 μm), and the durability and wear rates of the resulting composites were studied using ball-on-flat reciprocating tests. The results show that the impregnation technique is able to fill the surface pores with graphite, producing friction coefficients down to 0.06 in dry-sliding conditions and wear rates ranging from 10−4 to 10−7 (mm3/N-m). The main wear mechanism of the impregnated specimens was plastic deformation on the surface, which causes sealing of pores, while the wear of the counter-bodies was mainly abrasive. The durability of the lubricity regime is directly proportional to the amount of lubricant available as pores get sealed by the sliding action of the counter-body, so is proportional to the porosity.

Disclosure statement

No potential conflict of interest was reported by the author(s).

Additional information

Funding

The authors acknowledge the following Brazilian agencies for funding this research: CNPq, CAPES, Nidec Global Appliance, BNDES, and the Chilean agency ANID [grant number 72190023].

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