Determination of ethanol in blood using headspace gas chromatography with flameionization detector (HS-GC-FID): Validation of a method

References

• Chun, H.-J., Poklis, J. L., Poklis, A., & Wolf, C. E. (2016). Development and validation of a method for alcohol analysis in brain tissue by headspace gas chromatography with flame ionization detector. Journal of Analytical Toxicology, 40(August), 653–9. https://doi.org/10.1093/jat/bkw075
   PubMedGoogle Scholar
• De Martinis, B. S., & Martin, C. C. S. (2002). Automated headspace solid-phase microextraction and capillary gas chromatography analysis of ethanol in postmortem specimens. Forensic Science International, 128(3), 115–119. https://doi.org/10.1016/S0379-0738(02)00182-2
   PubMed Web of Science ®Google Scholar
• De Martinis, B. S., Martins Ruzzene, M. A., & Santos Martin, C. C. (2004). Determination of ethanol in human blood and urine by automated headspace solid-phase microextraction and capillary gas chromatography. Analytica Chimica Acta, 522(2), 163–168. https://doi.org/10.1016/j.aca.2004.07.007
   Web of Science ®Google Scholar
• Diana, D., Sorin, M., Cornelia, M., Elena, B., & Vasil, A.,. (2009). Development and validation of a quantitative determination method of blood ethanol by gas chromatography with headspace (GC-HS). Romanian Journal of Legal Medicine, 17(4), 303–308. doi: 10.4323/rjlm.2009.303
   Web of Science ®Google Scholar
• Görkem, M., Zeliha, K., Emrah, D., Vugar, A., Seda, K., Serap, Y., & Tülin,. (2010). Simultaneous headspace-GC – FID analysis for methanol and ethanol in blood, saliva, and urine: Validation of method and comparison of specimens. Journal of Chromatographyonline.com, 28(7), 540–544. http://www.chromatographyonline.com/
   Google Scholar
• Hong-tao, X., Lin, H., Rong-Sheng, T., Ji-Ying, Y., Lu, C., Jing, Z., Jin-qi, L., Yuan, B., & Yuan, Z., . (2014). Rapid and Sensitive Headspace Gas Chromatography-Mass spectrometery Method for the analysis of Ethanol in the whole Blood. Journal of Clinical Laboratory Analysis, 28(5), 386–390. https://doi.org/10.1002/jcla.21698
   PubMed Web of Science ®Google Scholar
• ICH. (2005). International conference on harmonization of technical requirements for registration of pharmaceuticals for human use topic Q2 (R1) validation of analytical procedures text and methodology. International Conference on Harmonization, 1994(November 1996), 1–17. https://www.gmp-compliance.org/guidemgr/files/Q2(R1).pdf
   Google Scholar
• Kovatsi, L., Giannakis, D., Arzoglou, V., & Samanidou, V. (2011). Development and validation of a direct headspace GC-FID method for the determination of sevoflurane, desflurane and other volatile compounds of forensic interest in biological fluids: Application on clinical and post-mortem samples. Journal of Separation Science, 34(9), 1004–1010. https://doi.org/10.1002/jssc.201000921
   PubMed Web of Science ®Google Scholar
• Lachenmeier, D. W. (2007). Rapid quality control of spirit drinks and beer using multivariate data analysis of Fourier transform infrared spectra. Food Chemistry, 101(2), 825–832. https://doi.org/10.1016/j.foodchem.2005.12.032
   Web of Science ®Google Scholar
• Magnusson, O. (2014). Eurachem guide: The fitness for purpose of analytical methods a laboratory guide to method validation and related topics. Eurachem Guide. Available from www.eurachem.org.
   Google Scholar
• Nikelly, J. G., & Betz, J. M. (1987). Determination of ethanol in alcoholic beverages by liquid chromatography using the UV detector. Journal of Chromatographic Science, 25(9), 391–394. https://doi.org/10.1093/chromsci/25.9.391
   PubMed Web of Science ®Google Scholar
• O’Neal, C. L., Wolf, C. E., Levine, B., Kunsman, G., & Poklis, A. (1996). Gas chromatographic procedures for determination of ethanol in postmortem blood using t-butanol and methyl ethyl ketone as internal standards. Forensic Science International, 83(1), 31–38. https://doi.org/10.1016/0379-0738(96)02007-5
   PubMed Web of Science ®Google Scholar
• Peters, F. T., Drummer, O. H., & Musshoff, F. (2007). Validation of new methods. Forensic Science International, 165(2–3), 216–224. https://doi.org/10.1016/j.forsciint.2006.05.021
   PubMed Web of Science ®Google Scholar
• Scientific Working Group for Forensic Toxicology, S. (2013). Standard practices for method validation in forensic toxicology. 37(7), 452-74. doi: 10.1093/jat/bkt054
   Google Scholar
• Snow, N. H., & Slack, G. C. (2002). Head-space analysis in modern gas chromatography. TrAC - Trends in Analytical Chemistry, 21(9–10), 608–617. https://doi.org/10.1016/S0165-9936(02)00802-6
   Web of Science ®Google Scholar
• Tiscione., N. B., IIene, A., Dustin Tate, Y., & Xiaoqin, S. (2011). Ethanol analysis by headSpace gas-chromatography with simultaneous flame ionization and mass spectrometery detection. Journal of Analytical Toxicology, 35(7), 501–511. https://doi.org/10.1093/anatox/35.7.501
   PubMed Web of Science ®Google Scholar
• Westland, J. L., & Dorman, F. L. (2013). Comparison of SPME and static headspace analysis of blood alcohol concentration utilizing two novel chromatographic stationary phases. Forensic Science International, 231(1–3), 50–56. https://doi.org/10.1016/j.forsciint.2013.05.007
   Web of Science ®Google Scholar
• Yarita, T., Nakajima, R., Otsuka, S., Ihara, T., Takatsu, A., & Shibukawa, M. (2002). Determination of ethanol in alcoholic beverages by high- performance liquid chromatography flame ionization detection using pure water as mobile phase. 976(1-2), 387–391. https://doi.org/10.1016/S0021-9673(02)00942-1
   Google Scholar
• Zuba, D., Parczewski, A., & Reichenbcher, M. (2002). Optimization of solid-phase microextraction conditions for gas chromatographic determination of ethanol and other volatile compounds in blood. Journal of Chromatography B: Analytical Technologies in the Biomedical and Life Sciences, 773(1), 75–82. https://doi.org/10.1016/S1570-0232(02)00143-5
   PubMed Web of Science ®Google Scholar