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Original Articles

Solvent-free one-pot synthesis and crystal structure of a spiro[indole-thiazine]

, , , &
Pages 201-207 | Received 18 Jun 2003, Accepted 20 Oct 2003, Published online: 13 May 2010
 

Abstract

An improved facile one-pot synthesis of 3′-(fluorophenyl)-spiro[3H-indole-3,2′-tetrahydro-1,3-thiazine]-2,4′(1H)-dione is reported using an environmentally friendly green chemistry procedure under microwave irradiation. The crystal structure of the reported compound has been determined by a X-ray diffraction. The molecule is largely planar and has cell parameters of a = 11.181(9) Å, b = 11.06(1) Å, c = 12.715(12) Å, α = 90°, β = 98.31(7)°, γ = 90°.

Acknowledgements

Financial assistance from CSIR and UGC New Delhi is gratefully acknowledged.

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