Food Additives & Contaminants: Part A, Volume 29, Issue 4 (2012)

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Food Additives & Contaminants: Part A, Volume 29, Issue 4 (2012)

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Ministério da Agricultura, Pecuária e Abastecimento do Brasil – Laboratórios Nacionais Agropecuários: Methods of analysis for residues and contaminants in the food chain

Editorial

Editorial
Brazilian Ministry of Agriculture, Livestock and Food Supply (MAPA): strategies to tackle chemical food safety issues
Bruno Le Bizec Prof, Dr, HDR
Page: 481
Published online: 09 Mar 2012
CitationforBrazilian Ministry of Agriculture, Livestock and Food Supply (MAPA): strategies to tackle chemical food safety issues | Full Text | PDF (47.7 KB)
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Foreword

The National Agricultural Laboratories of Brazil and the control of residues and contaminants in food
A. de Queiroz Mauricio & E.S. Lins
Pages: 482-489
Published online: 17 Nov 2011
AbstractforThe National Agricultural Laboratories of Brazil and the control of residues and contaminants in food | Full Text | References | PDF (350.5 KB)
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Original Articles

Article
Evolution of a residue laboratory network and the management tools for monitoring its performance
E.S. Lins, E.S. Conceição & A. De Q. Mauricio
Pages: 490-496
Published online: 14 Feb 2012
AbstractforEvolution of a residue laboratory network and the management tools for monitoring its performance | Full Text | References | PDF (1.3 MB)
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Article
β-lactam antibiotics residues analysis in bovine milk by LC-ESI-MS/MS: a simple and fast liquid–liquid extraction method
L. Jank, R.B. Hoff, P.C. Tarouco, F. Barreto & T.M. Pizzolato
Pages: 497-507
Published online: 11 Oct 2011
Abstractforβ-lactam antibiotics residues analysis in bovine milk by LC-ESI-MS/MS: a simple and fast liquid–liquid extraction method | Full Text | References | PDF (719.5 KB)
  • 739 Views
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Article
High-throughput multiclass screening method for antibiotic residue analysis in meat using liquid chromatography-tandem mass spectrometry: a novel minimum sample preparation procedure
M.S. Bittencourt, M.T. Martins, F.G.S. de Albuquerque, F. Barreto & R. Hoff
Pages: 508-516
Published online: 11 Oct 2011
AbstractforHigh-throughput multiclass screening method for antibiotic residue analysis in meat using liquid chromatography-tandem mass spectrometry: a novel minimum sample preparation procedure | Full Text | References | PDF (569 KB)
  • 558 Views
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Article
Validation of a quantitative and confirmatory method for residue analysis of aminoglycoside antibiotics in poultry, bovine, equine and swine kidney through liquid chromatography-tandem mass spectrometry
M.P. Almeida, C.P. Rezende, L.F. Souza & R.B. Brito
Pages: 517-525
Published online: 08 Nov 2011
AbstractforValidation of a quantitative and confirmatory method for residue analysis of aminoglycoside antibiotics in poultry, bovine, equine and swine kidney through liquid chromatography-tandem mass spectrometry | Full Text | References | PDF (908.3 KB)
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Article
Occurrence of antimicrobial residues in Brazilian food animals in 2008 and 2009
C.K.V. Nonaka, A.M.G. Oliveira, C.R. Paiva, M.P. Almeida, C.P. Rezende, C.G.O. Moraes, B.G. Botelho, L.F. Souza & P.G. Dias
Pages: 526-534
Published online: 30 Nov 2011
AbstractforOccurrence of antimicrobial residues in Brazilian food animals in 2008 and 2009 | Full Text | References | PDF (176.5 KB)
  • 415 Views
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Article
In-house validation of Premi®Test, a microbiological screening test with solvent extraction, for the detection of antimicrobial residues in poultry muscles
C.G. Magalhães, C.R. De Paiva, B.G. Botelho, A.M.G. De Oliveira, L.F. De Souza, C.V. Nonaka, K.V. Santos, L.M. Farias & M.A.R. Carvalho
Pages: 535-540
Published online: 07 Nov 2011
AbstractforIn-house validation of Premi®Test, a microbiological screening test with solvent extraction, for the detection of antimicrobial residues in poultry muscles | Full Text | References | PDF (135.7 KB)
  • 277 Views
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Article
Optimisation and validation of a quantitative and confirmatory LC-MS method for multi-residue analyses of β-lactam and tetracycline antibiotics in bovine muscle
C.P. Rezende, M.P. Almeida, R.B. Brito, C.K. Nonaka & M.O. Leite
Pages: 541-549
Published online: 10 Nov 2011
AbstractforOptimisation and validation of a quantitative and confirmatory LC-MS method for multi-residue analyses of β-lactam and tetracycline antibiotics in bovine muscle | Full Text | References | PDF (643.8 KB)
  • 638 Views
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Article
Determination and confirmation of chloramphenicol in honey, fish and prawns by liquid chromatography–tandem mass spectrometry with minimum sample preparation: validation according to 2002/657/EC Directive
Fabiano Barreto, Cristina Ribeiro, Rodrigo Barcellos Hoff & Teresa Dalla Costa
Pages: 550-558
Published online: 12 Jan 2012
AbstractforDetermination and confirmation of chloramphenicol in honey, fish and prawns by liquid chromatography–tandem mass spectrometry with minimum sample preparation: validation according to 2002/657/EC Directive | Full Text | References | PDF (444.6 KB)
  • 449 Views
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Article
Simultaneous determination of chloramphenicol and florfenicol in liquid milk, milk powder and bovine muscle by LC–MS/MS
D.R. Rezende, N. Fleury Filho & G.L. Rocha
Pages: 559-570
Published online: 12 Jan 2012
AbstractforSimultaneous determination of chloramphenicol and florfenicol in liquid milk, milk powder and bovine muscle by LC–MS/MS | Full Text | References | PDF (306.3 KB)
  • 657 Views
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Article
Producing a sulfamethazine quality control material under the framework of ISO/CD Guide 80
A.L. Cunha, P.F. Silva, E.A. Souza, J.R.A.M. Júnior, F.A. Santos & E.A. Vargas
Pages: 571-576
Published online: 13 Jan 2012
AbstractforProducing a sulfamethazine quality control material under the framework of ISO/CD Guide 80 | Full Text | References | PDF (164.4 KB)
  • 102 Views
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Article
Bioactivity-based screening methods for antibiotics residues: a comparative study of commercial and in-house developed kits
Rodrigo Hoff, Fabiana Ribarcki, Ivomar Zancanaro, Lara Castellano, Carolina Spier, Fabiano Barreto & Suzana Horta Fonseca
Pages: 577-586
Published online: 03 Jan 2012
AbstractforBioactivity-based screening methods for antibiotics residues: a comparative study of commercial and in-house developed kits | Full Text | References | PDF (320.6 KB)
  • 223 Views
  • 12 CrossRef citations
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Article
Optimisation and validation of a quantitative and confirmatory method for residues of macrolide antibiotics and lincomycin in kidney by liquid chromatography coupled to mass spectrometry
C.P. Rezende, L.F. Souza, M.P. Almeida, P.G. Dias, M.H. Diniz & J.C. Garcia
Pages: 587-595
Published online: 09 Feb 2012
AbstractforOptimisation and validation of a quantitative and confirmatory method for residues of macrolide antibiotics and lincomycin in kidney by liquid chromatography coupled to mass spectrometry | Full Text | References | PDF (445.2 KB)
  • 330 Views
  • 7 CrossRef citations
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Article
Validation of a rapid and sensitive routine method for determination of chloramphenicol in honey by LC–MS/MS
Tsuyoshi Taka, Marina C. Baras & Zahra F. Chaudhry Bet
Pages: 596-601
Published online: 23 Nov 2011
AbstractforValidation of a rapid and sensitive routine method for determination of chloramphenicol in honey by LC–MS/MS | Full Text | References | PDF (385 KB)
  • 440 Views
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Article
Validation of an LC-MS/MS method for malachite green (MG), leucomalachite green (LMG), crystal violet (CV) and leucocrystal violet (LCV) residues in fish and shrimp
Jociani Ascari, Sérgio Dracz, Flávio A. Santos, J.A. Lima, Maria Helena G. Diniz & Eugênia A. Vargas
Pages: 602-608
Published online: 10 Feb 2012
AbstractforValidation of an LC-MS/MS method for malachite green (MG), leucomalachite green (LMG), crystal violet (CV) and leucocrystal violet (LCV) residues in fish and shrimp | Full Text | References | PDF (172.6 KB)
  • 615 Views
  • 22 CrossRef citations
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Article
Development and validation of a method for Cd, Pb and As analysis in bovine, equine and poultry liver by inductively coupled plasma mass spectrometry
P.C.P. Lara, H.J.F. Fabrino, A. Germano & J.B.B. Da Silva
Pages: 609-616
Published online: 14 Oct 2011
AbstractforDevelopment and validation of a method for Cd, Pb and As analysis in bovine, equine and poultry liver by inductively coupled plasma mass spectrometry | Full Text | References | PDF (186 KB)
  • 231 Views
  • 1 CrossRef citations
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Article
Method validation for the determination of total mercury in fish muscle by cold vapour atomic absorption spectrometry
A.P. Nascimento Neto, L.C.S. Magalhães Costa, A.N.S. Kikuchi, D.M.S. Furtado, M.Q. Araujo & M.C.C. Melo
Pages: 617-624
Published online: 18 Jan 2012
AbstractforMethod validation for the determination of total mercury in fish muscle by cold vapour atomic absorption spectrometry | Full Text | References | PDF (252.4 KB)
  • 318 Views
  • 14 CrossRef citations
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Article
Method development for the control determination of mercury in seafood by solid-sampling thermal decomposition amalgamation atomic absorption spectrometry (TDA AAS)
D.P. Torres, M.B. Martins-Teixeira, E.F. Silva & H.M. Queiroz
Pages: 625-632
Published online: 03 Jan 2012
AbstractforMethod development for the control determination of mercury in seafood by solid-sampling thermal decomposition amalgamation atomic absorption spectrometry (TDA AAS) | Full Text | References | PDF (284.6 KB)
  • 425 Views
  • 22 CrossRef citations
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Article
Validation of an analytical method for the determination of cadmium (Cd) in fish by atomic absorption spectrometry with electrothermal atomisation
L.C.S.M. Costa, A.P.N. Neto, M.Q. Araújo, M.C.C. Melo, D.M.S. Furtado & A.N.S. Kikuchi
Pages: 633-640
Published online: 27 Feb 2012
AbstractforValidation of an analytical method for the determination of cadmium (Cd) in fish by atomic absorption spectrometry with electrothermal atomisation | Full Text | References | PDF (189.3 KB)
  • 257 Views
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Article
Within-laboratory validation of a multiresidue method for the analysis of 98 pesticides in mango by liquid chromatography-tandem mass spectrometry
N. Fleury Filho, C.A. Nascimento, E.O. Faria, A.R. Cruvinel & J.M. Oliveira
Pages: 641-656
Published online: 21 Oct 2011
AbstractforWithin-laboratory validation of a multiresidue method for the analysis of 98 pesticides in mango by liquid chromatography-tandem mass spectrometry | Full Text | References | PDF (1.1 MB)
  • 263 Views
  • 8 CrossRef citations
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Article
A multi-residue method for the determination of pesticides in high water content matrices by gas chromatography–single quadrupole mass spectrometry with electron ionisation (EI-GC/MS)
Mauro Lúcio Gonçalves de Oliveira, Fernando Diniz Madureira, Fabiano Aurélio, Ana Paula Pontelo, Gilsara Silva, Reginaldo Oliveira & Cláudia Paes
Pages: 657-664
Published online: 01 Feb 2012
AbstractforA multi-residue method for the determination of pesticides in high water content matrices by gas chromatography–single quadrupole mass spectrometry with electron ionisation (EI-GC/MS) | Full Text | References | PDF (494.8 KB)
  • 230 Views
  • 13 CrossRef citations
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Article
A multi-residue method for the determination of 90 pesticides in matrices with a high water content by LC–MS/MS without clean-up
Fernando Diniz Madureira, Fabiano Aurélio da Silva Oliveira, Wesley Robert de Souza, Ana Paula Pontelo, Mauro Lúcio Gonçalves de Oliveira & Gilsara Silva
Pages: 665-678
Published online: 07 Nov 2011
AbstractforA multi-residue method for the determination of 90 pesticides in matrices with a high water content by LC–MS/MS without clean-up | Full Text | References | PDF (754.6 KB)
  • 516 Views
  • 19 CrossRef citations
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Article
Modelling uncertainty estimation for the determination of aflatoxin M1 in milk by visual and densitometric thin-layer chromatography with immunoaffinity column clean-up
K.L. Carvalho, G.A.A. Gonçalves, A.L. Lopes, E.A. Santos, E.A. Vargas & W.F. Magalhães
Pages: 679-693
Published online: 03 Feb 2012
AbstractforModelling uncertainty estimation for the determination of aflatoxin M1 in milk by visual and densitometric thin-layer chromatography with immunoaffinity column clean-up | Full Text | References | PDF (383.7 KB)
  • 197 Views
  • 4 CrossRef citations
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Article
Co-occurrence of aflatoxins B1, B2, G1 and G2, ochratoxin A, zearalenone, deoxynivalenol, and citreoviridin in rice in Brazil
M.I. Almeida, N.G. Almeida, K.L. Carvalho, G.A.A. Gonçalves, C.N. Silva, E.A. Santos, J.C. Garcia & E.A. Vargas
Pages: 694-703
Published online: 08 Feb 2012
AbstractforCo-occurrence of aflatoxins B1, B2, G1 and G2, ochratoxin A, zearalenone, deoxynivalenol, and citreoviridin in rice in Brazil | Full Text | References | PDF (119.2 KB)
  • 654 Views
  • 101 CrossRef citations
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